scieee Science in your language
[en] (orig)

Tribological analysis of titanium alloy (Ti-6Al-4V) hybrid metal matrix composite through the use of Taguchi’s method and machine learning classifiers

Abstract

The preparation and tribological behavior of the titanium metal matrix (Ti-6Al-4V) composite reinforced with tungsten carbide (WCp) and graphite (Grp) particles were investigated in this study. The stir casting procedure was used to fabricate the titanium metal matrix composites (TMMCs), which had 8 weight percent of WCp and Grp. The tribological studies were designed using Taguchi's L27 orthogonal array technique and were carried out as wear tests using a pin-on-disc device. According to Taguchi's analysis and ANOVA, the most significant factors that affect wear rate are load and distance, followed by velocity. The wear process was ascertained by scanning electron microscopy investigation of the worn surfaces of the composite specimens. Pearson's heatmap and Feature importance (F-test) were plotted for data analysis to study the significance of input parameters on wear. Machine learning classification algorithms such as k-nearest neighbors, support vector machine, and XGBoost algorithms accurately classified the wear rate data, giving an accuracy value of 71.25%, 65%, and 56.25%, respectively.

Read accessible full text

Tribological analysis of titanium alloy (Ti-6Al-4V) hybrid metal matrix composite through the use of Taguchi’s method and machine learning classifiers

Author: Jatti, Vijaykumar S.
Publisher: Frontiers Media S.A.
Year: 2024
DOI: 10.3389/fmats.2024.1375200
Source: https://dspace.vsb.cz/bitstreams/788f91ba-68a5-40e2-8e8c-1e94b026bf79/download
TYPE O iginal Resea ch
PUBLISHED 12 Ap il 2024
DOI 10.3389/ ma s.2024.1375200
OPEN ACCESS
EDITED BY
Na ayan L.,
Sa ee ha Uni e si y, India
REVIEWED BY
Mahesh Shewale,
ASML, Uni ed S a es
Na een Venka esh S.,
Vello e Ins i u e o Technology (VIT), India
Subash Thanappan,
KAAF Uni e si y College, Ghana
*CORRESPONDENCE
Sachin Saluankhe,
[email p o ec ed]
RECEIVED 23 Janua y 2024
ACCEPTED 21 Ma ch 2024
PUBLISHED 12 Ap il 2024
CITATION
Ja i VS, Sawan DA, Deshpande R,
Saluankhe S, Cep R, Nas EA and
Mahmoud HA (2024), T ibological analysis o
i anium alloy (Ti-6Al-4V) hyb id me al ma ix
composi e h ough he use o Taguchi’s
me hod and machine lea ning classi ie s.
F on . Ma e . 11:1375200.
doi: 10.3389/ ma s.2024.1375200
COPYRIGHT
© 2024 Ja i, Sawan , Deshpande, Saluankhe,
Cep, Nas and Mahmoud. This is an
open-access a icle dis ibu ed unde he
e ms o he C ea i e Commons A ibu ion
License (CC BY). The use, dis ibu ion o
ep oduc ion in o he o ums is pe mi ed,
p o ided he o iginal au ho (s) and he
copy igh owne (s) a e c edi ed and ha he
o iginal publica ion in his jou nal is ci ed, in
acco dance wi h accep ed academic p ac ice.
No use, dis ibu ion o ep oduc ion is
pe mi ed which does no comply wi h
hese e ms.
T ibological analysis o i anium
alloy (Ti-6Al-4V) hyb id me al
ma ix composi e h ough he
use o Taguchi’s me hod and
machine lea ning classi ie s
Vijaykuma S. Ja i1, Dh u A. Sawan 1, Rashmi Deshpande2,
Sachin Saluankhe3*, Robe Cep4, Emad Abouel Nas 5and
Hai ham A. Mahmoud5
1Symbiosis Ins i u e o Technology, Symbiosis In e na ional Deemed Uni e si y, Pune, India,
2Depa men o Ins umen a ion Enginee ing, D Y Pa il Ins i u e o Technology, Sa i ibai Phule Pune
Uni e si y, Pune, India, 3Depa men o Biosciences, Sa ee ha School o Enginee ing, Sa ee ha
Ins i u e o Medical and Technical Sciences, Gazi Uni e si y Facul y o Enginee ing, Depa men o
Mechanical Enginee ing, Mal epe, Tü kiye, 4Depa men o Machining, Assembly and Enginee ing
Me ology, Facul y o Mechanical Enginee ing, VSB-Technical Uni e si y o Os a a, Os a a, Czechia,
5Depa men o Indus ial Enginee ing, College o Enginee ing, King Saud Uni e si y, Riyadh, Saudi
A abia
The p epa a ion and ibological beha io o he i anium me al ma ix (Ti-
6Al-4V) composi e ein o ced wi h ungs en ca bide (WCp) and g aphi e (G p)
pa icles we e in es iga ed in his s udy. The s i cas ing p ocedu e was used o
ab ica e he i anium me al ma ix composi es (TMMCs), which had 8 weigh
pe cen o WCp and G p. The ibological s udies we e designed using Taguchi’s
L27 o hogonal a ay echnique and we e ca ied ou as wea es s using a pin-
on-disc de ice. Acco ding o Taguchi’s analysis and ANOVA, he mos signi ican
ac o s ha a ec wea a e a e load and dis ance, ollowed by eloci y. The
wea p ocess was asce ained by scanning elec on mic oscopy in es iga ion o
he wo n su aces o he composi e specimens. Pea son’s hea map and Fea u e
impo ance (F- es ) we e plo ed o da a analysis o s udy he signi icance o
inpu pa ame e s on wea . Machine lea ning classi ica ion algo i hms such as k-
nea es neighbo s, suppo ec o machine, and XGBoos algo i hms accu a ely
classi ied he wea a e da a, gi ing an accu acy alue o 71.25%, 65%, and
56.25%, espec i ely.
KEYWORDS
i anium me al ma ix composi e, K-nea es neighbo ing, suppo ec o machine,
XGBoos , wea a e, ibology
1 In oduc ion
Ti anium alloys a e widely used in many echnical applica ions due o hei excellen
combina ion o high ha dness, wea esis ance, s eng h, co osion esis ance, s i ness,
and low densi y (Jiaoe al., 2018;Su eshe al., 2018;Cao and Liang, 2020). Ti anium
alloys a e widely u ilized o hei excep ional s eng h- o-weigh a io o lowe ene gy
consump ion, inc ease p oduc i i y, and ex end p oduc li e in he au omo i e, ae ospace,
spo s, anspo a ion, and medical equipmen indus ies (A a e al., 2018;Chaoe al.,
F on ie s in Ma e ials 01 on ie sin.o g
Ja i e al. 10.3389/ ma s.2024.1375200
2019;Pe undyu aiThanga ele al., 2020). Ti anium me al ma ix
composi es (TMMCs) can be b oadly classi ied in o wo ypes based
on he shape and dis ibu ion o ein o cemen s: con inuously
ein o ced TMMCs and discon inuously ein o ced TMMCs
(Guoe al., 2012;Jiaoe al., 2018;Haya e al., 2019). WC, Al2O3,
TiB, CNTs, SiC, FE3O4, B4C, TiC, G , and o he ce amic
pa icles and whiske s commonly ein o ce TMMCs (Lie al., 2015;
Zhange al., 2016;Sune al., 2020).
F a y e al. (F a ye al., 2003) epo ed ha he mechanical
and physical p ope ies o pu e i anium ein o ced wi h 10
weigh pe cen WP we e compa able o hose o he Ti-6Al-4V
(Ti64) alloy. A s udy by Choe e al. (Choee al., 2005a;Choee al.,
2005b) ound ha he size o he WP signi ican ly in luences
he mechanical cha ac e is ics o WP/Ti composi es. A ange o
mic os uc u es wi h good ensile s eng h and elonga ion we e
p oduced as a consequence o Wang e al.’s in es iga ions o he
a ied size dis ibu ion o TiC ein o cemen o i anium by DED
(Wange al., 2018). Using Ti/B4C composi e powde eeds ocks, Xia
e al. p oduced TiB + TiC ein o ced i anium in si u. They also
ho oughly examined he de elopmen o he in si u mic os uc u e
and he in e ac ion zone be ween he i anium and ce amic
ein o cemen (Xiae al., 2017).
Fu he mo e, in si u B4C/BN ein o ced Ti6Al4V composi es
we e s udied by Gup a e al. The main issue was wea pe o mance,
and s eng hening educed he sliding coe icien o ic ion (COF)
by hal compa ed o he Ti6Al4V ma ix (Gup ae al., 2018).
Using an in-si u app oach, Choi e al. p oduced hyb id composi es
o Ti6Al4V alloy wi h ein o cemen s TiB and TiC ha had a
cons an ein o cemen alloca ion. The esul s showed a signi ican
ela ionship be ween ein o cemen con en and mo e excellen
TMC wea esis ance, wi h mo e ein o cemen con en esul ing
in lowe wea loss (Kime al., 2011). A e elec oless pla ing o
manu ac u e coppe -coa ed CNTs, Wange al. (2017) used spa k
plasma sin e ing p ocedu es o c ea e coppe ma ix composi es.
The esul s showed ha elec oless pla ing signi ican ly imp o ed
he mechanical p ope ies by enhancing he elemen link be ween
coppe and ca bon nano ubes and enabling uni o m dispe sion
o CNTs.
By using elec oless nickel pla ing and SPS o c ea e composi es
o g aphi e lakes and coppe , Ren e al. d ama ically inc eased
he bonding a he g aphi e/coppe base con ac . Acco ding o
he indings, he bending cha ac e is ics and coe icien o he mal
expansion we e signi ican ly imp o ed by ins alling he NieP
ansi ion laye (Chene al., 2017). When 0.35w % o mul i-walled
ca bon nano ubes (MWCNTs) was added, Kondoh e al. disco e ed
ha he ensile pa ame e s, such as s eng h and yield, inc eased
by up o 27% and 42%, espec i ely, in con as o hose o pu e
i anium (Kondohe al., 2008). Wang e al. used an 823K sin e ing
empe a u e in conjunc ion wi h a spa k plasma sin e ing echnique
o c ea e a TMC composi e. The indings demons a ed ha when
he olume ac ion o MWCNTs eached 0.4 weigh pe cen , he
ma e ial’s comp essi e s eng h and yield s eng h bo h a ained
hei maximum alues. Then, when he MWCNT con en was aised
e en u he , he comp essi e s eng h d opped (Wange al., 2015).
Jin e al. s udied he p oduc ion o pu e i anium powde wi h
TiB2 ein o cing pa icles using a selec i e lase mel ing me hod.
All so s o wea cha ac e is ics, including adhesion, ab asion, and
oxida ion, we e imp o ed due o he Ti/TiB2 composi es (Jine al.,
2021). The i anium and Z O2 nanopa icle composi es ha Abd-
Elwahed e al. p oduced we e made ia powde me allu gy. The
esul s demons a ed ha aising he usual load imp o ed he
bonding, wea , and ic ion p ope ies, inc eased he o al amoun
o Z O2nanopa icles, and enhanced he sliding wea a e (Abd-
Elwahede al., 2020). An e al. assessed he ibological beha io s o
TMC coa ings a high empe a u es. The indings demons a e ha
delamina ion, plowing, and oxida ion wea p ocesses occu a 500C
oge he wi h inc eased wea a es o TMC coa ings (AnQie al.,
2019).
Rega ding ha dness and wea esis ance a oom empe a u e,
An e al.’s es s (Ane al., 2018;AnQ.e al., 2019) show ha he
hyb id TiBand TiC pa icles boos ed wi h i anium coa ing and
in e -g ow h ce amic s uc u es ou pe o m he TiB/Ti64 coa ing.
Fa ias concen a ed on how he ibological cha ac e is ics o
he TiC ein o cing pa icles wi h open po osi y in TMCs we e
a ec ed by spa k plasma sin e ing. The s udy’s indings e ealed
ha adding TiC pa icles enhanced ibological cha ac e is ics
like wea esis ance, coe icien o ic ion, and nano ha dness
(Fa íase al., 2019). Insu icien bonding be ween he ein o cemen
pa icles and ma ix migh cause ce amic pa icles o unc ion
as an ab asi e ma e ial, as pe he indings o Ram P abh
e al. The dimensions, mass, and mo phology o he al e na i e
phase ein o ced pa icles, he equi alen ma e ial, he load, he
mic os uc u e, he en i onmen , and he humidi y can all impac
he wea esis ance o composi e ma e ials (Rame al., 2014). Room
empe a u e esea ch was done by Huang Xie, who also ca ied
ou sliding wea ials on TMCs wi h mild s eel g ade 35. I on
oxide addi i es, independen o load, a ely imp o e he TMC’s
wea pe o mance because hey equi e lub ica ing capabili ies. The
MLG/Fe2O3 nanocomposi e and MLG wi h Fe2O3 mechanical
combina ion may signi ican ly imp o e he wea pe o mance
(Xiee al., 2021).
Zhou e al. examined he e ec o g aphene/Fe2O3
nanocomposi es on he ibological pe o mance o he TC11
alloy. They ound ha on he inju ed su ace, a hin, s able double
ibolaye consis ing o laye s p ima ily composed o MLG and
Fe2O3 was c ea ed, signi ican ly educing wea and ic ion. This
esea ch shows ha adding speci ic nanopa icles o ma e ials can
imp o e hei ibological p ope ies (Zhoue al., 2017). Ti anium
hyb id composi es wi h single and mul iple ein o cemen s we e
c ea ed by Lixia Xi e al. and ab ica ed using SLM. The hyb id
composi e esul se be ween he ein o cemen s and ma ix
gene a ed he in e acial s uc u e. The wea esis ance and CoF
cha ac e is ics a e enhanced when TiC and TiN ein o cemen
pa icles a e in oduced (Xie al., 2021).
P akash conside ed emo ing his p ope y lag. Ti anium alloy
(Ti-6Al-4V) is used o o i y bo on ca bide (B4C) ce amic pa icles
using powde me allu gy (PM). As a esul o his esea ch, a
newe composi e was c ea ed and es ed, imp o ing ha dness,
co osion esis ance, and educed densi y. The wea pe o mance
o he composi e specimens is mo e a ec ed by he applied loads
han by he amoun o B4C added. Scanning elec on mic oscopy
esul s demons a e ha he B4C- ein o ced Ti-6Al-4V composi e
has be e wea esis ance han he un ein o ced Ti alloy and
shows signs o mildly wo n su aces (Soo yaP akashe al., 2016).
Hu in es iga ed and analyzed he quali y o he componen s, he
p ocesses by which mic os uc u es o m, and he e icacy o
F on ie s in Ma e ials 02 on ie sin.o g
Ja i e al. 10.3389/ ma s.2024.1375200
wo kpiece wea in TiB- ein o ced Ti ma ix composi es, which
we e p oduced using he LENS app oach. The esul s sugges
ha TiB-TMCs, wi h hei inno a i e mic os uc u es and TiB
ein o cemen , exhibi ed supe io wea pe o mance compa ed
o bulk componen s composed o comme cially pu e i anium.
Fu he mo e, by a ying he lase powe , he cha ac e is ics o he
p oduced componen s we e imp o ed wi h ewe in e nal de ec s,
leading o be e wea pe o mance (Hue al., 2017). Using i anium
alloy ein o cemen o imp o e he g apheme’s ul ima e comp essi e
s eng h, ensile s eng h, wea esis ance, he mal conduc i i y, and
di usi i y, Gu buz e al. in es iga ed he p ope ies o ibological,
mechanical, and he mal aspec s (Gü büze al., 2021).
Measu ing he pa icula wea a e is c ucial o he ma e ial
selec ion and op imiza ion p ocess. Enginee s can choose he bes
ma e ials o a gi en applica ion by compa ing he wea a es o
se e al magnesium o magnesium alloys wi h o he ma e ials.
This is especially c ucial in sec o s like manu ac u ing, ae ospace,
and au omo i e, whe e wea esis ance signi ican ly impac s he
longe i y and dependabili y o componen s. A i icial In elligence
(AI) has yielded many bene i s and made signi ican s ides
in se e al indus ies, including manu ac u ing and heal hca e.
A i icial in elligence (AI) has shown o be ex emely use ul
in he medical indus y o asks including disease diagnosis,
he apy planning, medica ion de elopmen , and pa ien moni o ing
(Ma hews, 2019;Buccinoe al., 2023a;Buccinoe al., 2023b;
Yange al., 2023). A ype o a i icial in elligence called machine
lea ning algo i hms has been widely used o e alua e complex
medical da a, spo ends, and gene a e p ecise o ecas s. As a esul ,
he e has been an imp o emen in he p ecision o diagnoses, he
c ea ion o cus omized ea men p og ams, and he gene al quali y
o pa ien ca e.
Simila ly, AI has conside ably changed ope a ions in he
manu ac u ing sec o by acili a ing p edic i e main enance,
inc easing p oduc i i y, and s eamlining p ocedu es (Malekie al.,
2022;Malekie al., 2023). Demand o ecas ing, supply chain
op imiza ion, au oma ion, and quali y con ol ha e all bene i ed
om using machine lea ning algo i hms. These applica ions ha e
imp o ed ope a ional e ec i eness, lowe ed p oduc ion cos s,
and imp o ed p oduc quali y. The in eg a ion o E olu iona y
Compu ing wi h Machine Lea ning algo i hms has ecei ed e y
li le esea ch a en ion despi e he ema kable ad ancemen s in
AI and Machine Lea ning. E olu iona y compu ing is a sub ield
o a i icial in elligence ha uses me hods om na u al e olu ion,
including gene ic algo i hms, pa icle swa m op imiza ion, and
an colony op imiza ion, o ackle challenging op imiza ion
issues. Combining machine-lea ning echniques and e olu iona y
compu ing has excellen p omise in se e al ields. Resea che s
can mo e e ec i ely handle complex op imiza ion and p edic ion
asks by combining he adap i e sea ch capabili ies o E olu iona y
Compu ing wi h he lea ning and p edic i e powe s o Machine
Lea ning algo i hms. This in eg a ion can be u he implemen ed
in a ious ma e ial science and manu ac u ing domains
(Dhunganae al., 2019;Dhunganae al., 2021;Sadeke al., 2021;
Dhunganae al., 2022;Mish a and Ja i, 2023a;Dhunganae al.,
2023;G ecoe al., 2023). This hyb id echnique can help ind he
bes solu ions in complex p oblem spaces, inc ease he p ecision
and e ec i eness o op imiza ion algo i hms, and imp o e ea u e
selec ion in machine-lea ning models.
Es ima ing he p ecise wea a e o Hyb id Me al Ma ix
Ti anium alloy is essen ial in sec o s whe e wea esis ance is
a i al componen . While machine lea ning has demons a ed
po en ial in p edic i e modeling, e alua ing hei pe o mance
and choosing which algo i hm wo ks bes o his pa icula
use case is necessa y. Fu he mo e, he e needs o be a mo e
ho ough analysis and compa ison o a ious algo i hms and a
pauci y o esea ch in his a ea. Thus, compa ing he e ec i eness
o machine lea ning algo i hms, namely K-Nea es Neighbou ing
(KNN), Suppo Vec o Machine (SVM), and XGBoos classi ica ion
in o ecas ing he p ecise wea a e o he Hyb id Me al Ma ix
Ti anium alloy is he opic his esea ch s udy a emp s o add ess.
This s udy used he s i cas ing me hod o c ea e a i anium alloy,
Ti-6Al-4V, wi h ein o cemen s made o ungs en ca bide (WC) and
g aphi e (G ) hyb id me al ma ix composi e. P ocess a iables like
load, sliding eloci y, sliding dis ance, and ibological expe imen s
we e pe o med based on he Taguchi L27 o hogonal a ay.
2 Ma e ials and me hods
The p ima y ma ix ma e ial used was he i anium alloy Ti-
6Al-4V; Table1 shows he chemical composi ion o he ma ix
alues o his alloy. The pa icles ein o ced wi h WC and G ha e
been selec ed. The a e age size o he g aphi e pa icles was 25μm,
whe eas he WC pa icles we e 45μm. The equi ed amoun o Ti-
6Al-4V i anium alloy was mel ed in a g aphi e c ucible using an
elec ical u nace. The ein o cing pa icles we e hea ed o 500°C o
emo e he mois u e. A speci ic quan i y o ein o cing pa icles was
mixed wi h he i anium alloy. The hyb id composi e ma e ial was
egula ly blended. A e he hyb id composi e was inse ed in o he
p epa ed die a 800°C, i was le o solidi y a oom empe a u e.
The sample’s mic os uc u es and wo n su aces we e examined
using op ical and scanning elec on mic oscopy. Mic oha dness
es e o model-Mic oha dness es e om OMNI ech, MVH-1
au oma ic es load 10gm o 1,000gm employed o mic oha dness
measu emen . As indica ed in Figu e1, he composi e specimens’
d y sliding wea quali ies we e e alua ed using he DUCOM pin-
on-disc sliding wea es ing appa a us (Manu ac u e : DUCOM,
Bangalo e, India). The ASTM G99-95 ules we e ollowed when
conduc ing he d y sliding wea es ing. The pin was cleaned wi h
ace one, and i s ini ial mass was measu ed wi h a digi al elec onic
balance. A e ha , he pin was held up agains a e ol ing EN-32
s eel disk (coun e ace) wi h 65 HRC ha dness h oughou he es .
Figu e2A,B depic s he cas ed and machined samples, espec i ely.
Th oughou he es ing, adjus men s we e made o he dis ance,
eloci y, and a e age load. A he end o each es , he pin’s ul ima e
mass was measu ed a e being cleaned wi h ace one. We calcula ed
he mass loss o he pin due o sliding wea by aking he di e ence
be ween i s ini ial and inal masses. The olume loss owing o wea
was calcula ed using he densi y alues linked wi h he pin. Nex , he
wea a e o he composi e pins was asce ained.
The ollowing is he p ocess o ca ying ou he wea es :
Fi s , he es sample is ca e ully weighed on a s a e-o - he-a
digi al balance, and i s o iginal mass is eco ded. The specimen is
hen secu ely secu ed using he no ch, and i s su ace is posi ioned so
ha i makes con ac wi h he disk. The ack adius is hen modi ied
o mee he unique equi emen s o he es . Following p ope
F on ie s in Ma e ials 03 on ie sin.o g
Ja i e al. 10.3389/ ma s.2024.1375200
TABLE 1 Chemical composi ion o Ti6Al4V.
Alloying elemen s Ti Al V Fe O N C
Chemical con en (w %) 85.096 7.75 6.5 0.34 0.02 0.04 0.05
FIGURE 1
Wea es on disc (Mish a and Ja i, 2023b;Mish ae al., 2023)
FIGURE 2
(A) Cas wea pins. (B) Machined wea pins.
specimen posi ioning speci ied no mal loads a e supplied, and he
sliding eloci y is se in compliance wi h he es pa ame e s. The
es is hen un o co e he speci ied dis ance o e a compu ed ime
in e al. Fo e e y es , he pin olume loss was de e mined using
he pin-heigh loss me hod. Each es was conduc ed h ee imes o
gua an ee epea abili y, and he a e age o he h ee es s was used
o de e mine he wea a e using Eq.(1). This p ocess is epea ed
o o he specimens wi h a ying olume pe cen ages and could be
F on ie s in Ma e ials 04 on ie sin.o g
Ja i e al. 10.3389/ ma s.2024.1375200
TABLE 2 Inpu p ocess pa ame e s.
Le el Sliding
speed (m/s)
Load (N) Sliding
dis ance (m)
1 2 20 500
2 4 30 1,000
3 6 40 1,500
es ed unde a ious condi ions. This me hod makes i possible o
compa e wea cha ac e is ics unde a ious ci cums ances.
The wea pa ame e s chosen o he es ing based on machine
capaci y, li e a u e analysis, and pilo ials a e shown in Table2.
Pilo expe imen s we e conduc ed o asce ain he p ac ical limi s o
he p e iously indica ed pa ame e s necessa y o he wea o occu
in a s eady s a e. Re e ing o ASTM G99-95, he pin used in he wea
es is 30mm long and has an 8mm diame e .
Wea a e(mm3/Nm)=(Volumeloss∗Ha dness)/
(No malLoad∗Slidingdis ance)(1)
The Taguchi echnique aims o minimize a ia ion in a p ocess
h ough obus expe imen design. The main objec i e o he
p ocedu e is o p o ide he make wi h high-quali y ou pu a a low
cos . D . Genichi Taguchi o Japan de eloped he Taguchi me hod
and has pe sis ed in using ha a ia ion. Thus, bo h he p oduce
and socie y a e impac ed by low p ocess quali y. He de eloped
a sys em o designing expe imen s o in es iga e how di e en
pa ame e s a ec he mean and a iance o a p ocess pe o mance
cha ac e is ic ha shows how well he p ocess is doing.
Taguchi’s expe imen al design ga he s he necessa y da a o
iden i y he a iables signi ican ly in luencing p oduc quali y
wi h mino expe imen a ion, sa ing ime and esou ces. This is
accomplished using o hogonal a ays o o ganize he a iables
in luencing he p ocedu e and he magni udes a which hey should
be shi ed. Key p ocess ac o s we e iden i ied using analysis o
a iance. An L27 o hogonal a ay was chosen o he cu en
expe imen , as indica ed in Table3.
This s udy classi ies and p edic s he wea a e o hyb id
me al ma ix composi e using KNN, SVM, and XG Boos machine
lea ning classi ica ion echniques. To build a con usion ma ix and
AUC-ROC cu es o u he in-dep h analysis and o p ecisely
assess he wea a e using classi ica ion, sample da a was cons uc ed
using a syn he ic da a gene a ion ool in MATLAB based on
he expe imen al da a. The classi ica ion me hod is a supe ised
lea ning echnique ha ca ego izes new obse a ions using aining
da a. Using he da ase o supplied obse a ions, a p og am lea ns
how o ca ego ize esh obse a ions in o a ious classes o g oups
in he classi ica ion p ocess. The da a in he cu en s udy is di ided
in o wo g oups acco ding o whe he he alue exceeds o alls sho
o he 0.084 a e age o all wea a e alues. The con usion ma ix
was plo ed using he Py hon me ics module om he sklea n
package. In o de o achie e p ecise ou comes o da a p edic ion,
he da ase was spli in o wo sec ions: 80 pe cen o aining da a and
20 pe cen o andom es da a. The con usion ma ix is composed
o h ee ypes o da a: False posi i es (FP) and False nega i es (FN),
which e lec w ongly o ecas ed da a o sugges ha he e was an
e o in he p edic ion p ocess; and T ue posi i es (TP) and T ue
nega i es (TN), which ep esen success ully an icipa ed da a. K-
old (k = 1) was conside ed o he numbe o neighbo s (k), and
KNN, SVM, and XGBoos classi ica ion was pe o med o ob ain
a wide ange o classi ica ion da a. Pea son’s hea map analysis and
ea u e impo ance plo (F- es ) we e plo ed u he o unde s and
he signi icance o ea u es on wea loss. A lowcha explaining
hea map analysis is depic ed in Figu e3.
The cu en s udy uses a k-nea es neighbo (kNN) classi ica ion
me hod, which inds he closes Euclidean dis ance be ween he
a e age alue and each wea a e alue ( e e o Figu e4A).
Fo he kNN classi ica ion me hod, he e a e a ious ypes o
hype pa ame e op ions, such as:
a) The numbe o neighbo s decides he numbe o nea es
neighbo s o classi y each alue o poin in he a ge da ase .
b) Dis ance me ic, which is used o measu e dis ance be ween
2 poin s.
c) Dis ance weigh decides whe he he dis ance is equal o
in e se (1/dis ance).
SVMs we e c ea ed o sol e bina y classi ica ion issues. Howe e ,
when compu a ionally demanding mul iclass p oblems become
mo e common, se e al bina y classi ie s a e buil and coupled o
c ea e SVMs ha can ca y ou hese mul iclass classi ica ions using
bina y me hods. The SVM classi ie unc ion (SVC) is de ined
using inpu pa ame e s like he ype o ke nel used, he ma gin,
and he hype plane. Once he da a is ained using he SVM
classi ie unc ion, he es da a is p edic ed based on he ained and
alida ed da a. The wo k low o he SVM classi ica ion algo i hm is
depic ed in Figu e4B. XGBoos is a scalable and accu a e g adien -
boos ing solu ion ha pushes he compu a ional bounda ies o
boos ed ee algo i hms, p ima ily accele a ing compu a ional speed
and machine lea ning model pe o mance. As pa o an ensemble
app oach mean o p oduce supe io p edic ions wi h imbalanced-
class da a, Ex eme G adien Boos ing, o XGBoos , has become
inc easingly popula as a p edic ion algo i hm in ecen yea s.
XGBoos classi ica ion is simila o he F- es as i selec s he bes
ea u es o p edic he da a a e i ains and alida es he aining
da ase . I con inues un il he bes ea u e, which has he mos
signi icance on he da a, is selec ed, and no ea u es emain in
he da ase o e alua e. The wo k low o he XGBoos classi ica ion
algo i hm is depic ed in Figu e4C. The alues a e eco ded a e he
da ase is collec ed using wea loss expe imen s. Hea map analysis
and F- es a e done o iden i y he mos signi ican ea u es o he
da ase . Then, supe ised machine lea ning algo i hms, in his case,
classi ica ion algo i hms like kNN, SVM, and XGBoos , a e used o
classi y he da a based on he aining and alida ion da ase , and
he da a is p edic ed using he ained model. The esul s a e hen
analyzed o he bes wea loss a e based on he bes ea u es.
3 Resul s and discussions
In o de o es ima e he p ecise wea a e o hyb id composi es,
his sec ion p esen s he wea a e esul s oge he wi h s a is ical
analysis and a machine lea ning echnique. The expe imen al
pa ame e s used o he s udies a e shown in Table3, oge he wi h
he co esponding obse ed wea a e alues.
F on ie s in Ma e ials 05 on ie sin.o g

Ja i e al. 10.3389/ ma s.2024.1375200
TABLE 3 Expe imen al layou wi h obse ed alues.
S. No. Load (N) Veloci y (m/s) Dis ance (m) Wea a e (mm3/N-mm)
1 20 2 500 0.00021959
2 20 2 500 0.00026440
3 20 2 500 0.00044366
4 20 4 1,000 0.00018150
5 20 4 1,000 0.00009635
6 20 4 1,000 0.00015909
7 20 6 1,500 0.00056914
8 20 6 1,500 0.00007618
9 20 6 1,500 0.00004332
10 30 2 500 0.00014341
11 30 2 500 0.00028083
12 30 2 500 0.00024797
13 30 4 1,500 0.00007569
14 30 4 1,500 0.00006075
15 30 4 1,500 0.00006672
16 30 6 500 0.00017328
17 30 6 500 0.00024498
18 30 6 500 0.00023602
19 40 2 1,500 0.00006797
20 40 2 1,500 0.00005676
21 40 2 1,500 0.00007618
22 40 4 500 0.00023751
23 40 4 500 0.00011876
24 40 4 500 0.00014341
25 40 6 1,000 0.00010531
26 40 6 1,000 0.00009635
27 40 6 1,000 0.00004369
3.1 S a is ical analysis
The d y sliding wea es was pe o med using pin-on-disc
equipmen . The analysis o a iance and signal- o-noise (S/N) a io
echniques we e used o de e mine he signi ican pa ame e s. The
S/N a ios a e used o e alua e how noise ac o s a ec pe o mance
me ics. Th ee S/N a ios a e ypical and equen ly u ilized; hey
e alua e he deg ee o a ia ion in he answe da a and he deg ee
o which he a e age esponse esembles he a ge . Theo e ically,
highe , smalle , and be e a e he be e o hem. Smalle is
be e . The guideline was applied in his s udy o educe wea a e.
The signal- o-noise a io, o S/N a io, gauges he suscep ibili y
o he quali y a ibu e unde s udy o expe imen ally induced
uncon ollable e en s.
F on ie s in Ma e ials 06 on ie sin.o g
Ja i e al. 10.3389/ ma s.2024.1375200
FIGURE 3
Hea map lowcha .
FIGURE 4
(A) kNN classi ica ion lowcha . (B) SVM classi ica ion lowcha . (C) XG-Boos classi ica ion lowcha .
TABLE 4 Analysis o a iance o wea a e.
Sou ce DF Seq SS Adj SS Adj MS F P
Load (N) 2 0.0000001 0.0000001 0.0000001 3.31 0.057
Veloci y (m/s) 2 0.0000001 0.0000001 0.0000001 0.49 0.622
Dis ance (m) 2 0.0000001 0.0000001 0.0000001 3.35 0.056
E o 20 0.0000002 0.0000002 0.0000002
To al 26 0.0000004
An analysis o a iance (ANOVA) was pe o med o in es iga e
he e ec s o load, eloci y, and dis ance on he wea a e;
he esul s a e shown in Table4. The load and he dis ance
subs an ially impac ed he wea a e, acco ding o he F- es and
p- alue esul s. Table5 and Table6 depic he esponse able
o signal- o-noise a ios and means, espec i ely. As pe he
esul s, he load ollowed by dis ance and eloci y a ec s he
wea a e.
Figu e5A displays he plo o he wea a e’s p ima y in luence. I
is e iden ha he wea a e ends o inc ease wi h highe eloci ies
and no mal loads. Fu he mo e, Figu e5B illus a es he wea a e
in e ac ion plo . The lines in e sec o e eal a s ong in e ac ion
e ec be ween he wea a e and he load and eloci y, load and
dis ance, and eloci y and dis ance.
Figu e5C displays a esidual plo o he pa icula wea a e.
A s anda d p obabili y plo deno es a no mal dis ibu ion o he
F on ie s in Ma e ials 07 on ie sin.o g
Ja i e al. 10.3389/ ma s.2024.1375200
TABLE 5 Response able o signal- o-noise a ios.
Le el Load (N) Veloci y (m/s) Dis ance (m)
1 71.94 75.31 72.70
2 76.40 78.33 78.88
3 79.96 74.66 78.78
Del a 8.02 3.67 6.18
Rank 1 3 2
TABLE 6 Response able o means.
Le el Load (N) Veloci y (m/s) Dis ance (m)
1 0.000228 0.000200 0.000229
2 0.000170 0.000127 0.000114
3 0.000105 0.000176 0.000116
Del a 0.000123 0.000073 0.000116
Rank 1 3 2
esiduals. The e was no e idence o da a skewness o ou lie s in
he his og am plo . The e we e no appa en pa e ns in he esidual
e sus o de ed plo o he esidual e sus i ed plo . These indings
imply ha di e ences in ime o en i onmen al condi ions did no
cause any inaccu acies in he da a ga he ing.
The wea a e indica es he amoun o ma e ial loss o
wea olume pe uni o sliding dis ance and uni load. Se e al
wea egimes we e ound in he wea map by analyzing he
wea a e alues. A di e en combina ions o sliding eloci ies
and no mal loads, hese wea egimes o e insigh s in o he
p edominan wea mechanisms, including adhesi e wea , ab asi e
wea , delamina ion, plas ic de o ma ion, oxida ion, and mel ing.
Changes in wea a e o e ela i ely modes di e ences in
pa ame e s like a e age load, sliding eloci y, empe a u e, and ime
a e e e ed o as wea ansi ions. Wea ansi ion cha s usually
iden i y and cha ac e ize a ious wea egimes o mechanisms. Low
wea a es and mild con ac condi ions wi h a mix o adhesi e
and oxida i e wea p edomina e a e cha ac e is ics o he mild
wea egime. On he o he hand, he se e e wea egime is
cha ac e ized by ele a ed wea a es and usually a ises om mo e
igo ous wo king ci cums ances. Nume ous mechanisms, including
ab asi e wea , plowing, and delamina ion, can con ibu e o
se e e wea .
Plowing emo es ma e ial due o he in e ac ion o mic oscopic
aspe i ies on one su ace wi h ano he , which causes ab asi e wea .
Rough su aces o he p esence o ha d pa icles a e linked o his
mechanism. Oxida i e wea is caused by he in e ac ion o he
alloy wi h ambien oxygen, p oducing oxide laye s on he alloy
su ace. Inc eased wea a e and su ace de e io a ion may esul
om his mechanism. The e m “delamina ion” desc ibes how laye s
FIGURE 5
(A) Main e ec s plo o wea a e. (B) In e ac ion plo o wea a e. (C)
Residual plo s o wea a e.
come away om he su ace o a subs ance. I equen ly happens
in a eas wi h a concen a ion o localized ension, which causes
wea deb is and su ace oughness o accumula e. This phenomenon
is known as plas ic de o ma ion, when a ma e ial de o ms and
lows due o an applied a e age load. A wo-dimensional g aph
o he wea a e alues is displayed in Figu es6A–C. The colo
ep esen ed he wea a e alues. This image made he analysis
o wea a e a ia ions unde a ious es se ings possible. These
wea maps help de e mine p e ailing wea egimes, comp ehend
he wea mechanisms, and choose he bes ma e ials and ope a ing
se ings o speci ic applica ions. This in es iga ion ound ha he
wea a e dec eased a lowe eloci y and load alues and inc eased
F on ie s in Ma e ials 08 on ie sin.o g
Ja i e al. 10.3389/ ma s.2024.1375200
FIGURE 6
(A) Con ou plo o wea a e e sus load, eloci y. (B) Con ou plo o
wea a e e sus load, dis ance. (C) Con ou plo o wea a e e sus
eloci y, dis ance.
a highe eloci y and load alues. The wea map’s a ied colo ed
zones co espond o dis inc wea a es a a ying eloci ies and
loads. The ansi ion lines we e used o de ine he zones by he
expe imen al se up.
The ideal eloci y and load combina ion ha educes wea a e
can be ound h ough wea map analysis, making i possible o
iden i y ope a ing si ua ions whe e he ma e ial exhibi s excellen
wea pe o mance. This knowledge is a e e ence o echnical
applica ions using he hyb id me al ma ix composi e alloy. This is
especially impo an in he au omo i e, ae ospace, and biomedical
indus ies, whe e wea esis ance is c i ical. Fo he p esen s udy, he
wea a e is lowe be ween 3.5 and 4.5m/s eloci y and 25N–35N
load; see Figu es6A,B shows ha he wea a e is lowe be ween
27.5 N and 40N load and 1,000m–1,500m dis ance. Figu e6C
shows ha he wea a e is lowe be ween 2 and 4.5m/s eloci y and
1,250m–1,500m dis ance.
3.2 Op ical and SEM analysis
The op ical mic og aph o he composi e is shown in Figu e7A.
The sample has excellen compac ness and is ee o mic o- issu es
and po es. The WCp-G p ein o cemen was e enly dis ibu ed
h oughou he composi es o pe mi i s p esence in he Ti-6Al-4V
ma ix. The Ti-6Al-4V ma ix has uni o mly dis ibu ed iny WCp-
G p ein o cemen s, e en hough Ti anium Composi es In e ac ion
does no obse e any eac ions. I is impo an o no e ha
WCp and G p do no combine o o m a s aigh o wa d bina y
combina ion bu p oduce a new in e ace s uc u e. The a e age
alue o Vicke s Mic oha dness o he hyb id composi e ob ained
using a mic oha dness es e is 892 VHN.
SEM analysis o he wea su aces de eloped in o d y sliding
wea in he s eady s a e egime p o ides a c ucial ool o accu a ely
cha ac e izing he wea beha io o he composi es. Figu e7B shows
he composi es’ wo n-ou su ace ollowing wea . The ex ao dina y
ha dness o he composi e means ha he wo n-ou su aces a e
ba ely pe cep ible. This example has a e y smoo h su ace because
he WCp and GRp ein o cemen pa icles a e secu ely bonded o
he ma ix phase a ha le el. I is also clea ha ein o cemen s
ha e no wo n down only a li le. The sel -lub ica ing ac ion o
he ibo su ace ein o cemen s causes his. The wo n su ace
o he composi e makes he p esence o lamina ed laye s qui e
e iden . In his pic u e, he laye has changed he easily obse able
sliding su ace. The su aces also appea smoo h because o he
ein o cing componen .
3.3 Wea a e p edic ion using machine
lea ning classi ie
Da a was ca ego ized using machine lea ning based on he
ape angle o he squa e slo s in he s ainless s eel pla e. Using
Py hon lib a ies, Pea son’s hea map and F- es plo s we e c ea ed
o de e mine he ea u e impo ance o inpu pa ame e s, including
load, eloci y, and dis ance. Pea son’s hea map analysis is plo ed as
shown in Figu e8A, which depic s he minimal signi icance o load
and eloci y on he wea a e.
As shown in Figu e8B, a ea u e is deemed insigni ican i i s
F- es alue is below he F-dis ibu ion alue. Howe e , any F- es
alue o an inpu pa ame e o e he c i ical F-dis ibu ion will be
ega ded as a signi ican ea u e o inpu pa ame e . The k-nea es
Neighbo s (kNN) me hod p edic s he label o alue o a new da a
poin by conside ing he labels o alues o i s k-nea es neighbo s
in he aining da ase . In he cu en analysis o wea loss, he
alues below he a e age alue o wea loss we e conside ed as 1,
and he alues abo e he a e age alue we e conside ed as 0, e e o
Figu e9A. Wea loss should be minimal as i will gi e be e esul s.
The p edic ion accu acy o he kNN classi ica ion o wea loss was
71.25%, e e o Table7.
F on ie s in Ma e ials 09 on ie sin.o g