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Relationship of time-dependent parameters from destructive and non-destructive tests of structural concrete

Lehner, Petr

Abstract

Reinforced concrete structures are typically exposed to a combination of aggressive substances and mechanical stresses, which contribute to fast degradation. The present research was conducted to evaluate five time-dependent parameters from several different tests, namely compressive strength, static modulus, dynamic modulus, surface, and bulk electrical resistance. Some parameters were obtained using destructive testing (DT) and some using non-destructive testing (NDT). Due to the correlation and calculation of regression curves, it was possible to compare the correlation of parameters important for estimating the durability of reinforced concrete structures in relation to degradation and corrosion. Concrete of C40/50 grade was examined in several time periods, and the parameter relationships were analysed. At the same time, a statistical evaluation was carried out, and therefore the study contains the average values and standard deviations of all measured parameters. The results show that the compressive strength and the electrical resistivity of the surface and bulk have a high correlation. In contrast, the dynamic modulus and electrical resistivity have low linear correlation, but it was possible to apply a quadratic curve with a high degree of fit. For the comparison of static elastic modulus and electrical resistance, the quality of the quadratic regression model was low but sufficient. The results show that, for structural concrete, the presented NDT methods can be used to estimate other parameters obtained from the DT methods.

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  Ci a ion: Lehne , P.; H abo á, K. Rela ionship o Time-Dependen Pa ame e s om Des uc i e and Non-Des uc i e Tes s o S uc u al Conc e e. Ma hema ics 2022,10, 460. h ps://doi.o g/10.3390/ ma h10030460 Academic Edi o s: Theodo e E. Simos and Cha alampos Tsi ou as Recei ed: 31 Decembe 2021 Accep ed: 29 Janua y 2022 Published: 30 Janua y 2022 Publishe ’s No e: MDPI s ays neu al wi h ega d o ju isdic ional claims in published maps and ins i u ional a il- ia ions. Copy igh : © 2022 by he au ho s. Licensee MDPI, Basel, Swi ze land. This a icle is an open access a icle dis ibu ed unde he e ms and condi ions o he C ea i e Commons A ibu ion (CC BY) license (h ps:// c ea i ecommons.o g/licenses/by/ 4.0/). ma hema ics A icle Rela ionship o Time-Dependen Pa ame e s om Des uc i e and Non-Des uc i e Tes s o S uc u al Conc e e Pe Lehne 1,* and K is ýna H abo á2 1Depa men o S uc u al Mechanics, Facul y o Ci il Enginee ing, VSB—Technical Uni e si y o Os a a, L. Podéš ˇe 1875, Po uba, 70800 Os a a, Czech Republic 2Ins i u e o Building Tes ing, Facul y o Ci il Enginee ing, B no Uni e si y o Technology, Ve eˇ í331/95, 60200 B no, Czech Republic; k is yna.h abo a@ u b .cz *Co espondence: pe [email p o ec ed] Abs ac : Rein o ced conc e e s uc u es a e ypically exposed o a combina ion o agg essi e sub- s ances and mechanical s esses, which con ibu e o as deg ada ion. The p esen esea ch was conduc ed o e alua e i e ime-dependen pa ame e s om se e al di e en es s, namely com- p essi e s eng h, s a ic modulus, dynamic modulus, su ace, and bulk elec ical esis ance. Some pa ame e s we e ob ained using des uc i e es ing (DT) and some using non-des uc i e es ing (NDT). Due o he co ela ion and calcula ion o eg ession cu es, i was possible o compa e he co ela ion o pa ame e s impo an o es ima ing he du abili y o ein o ced conc e e s uc u es in ela ion o deg ada ion and co osion. Conc e e o C40/50 g ade was examined in se e al ime pe iods, and he pa ame e ela ionships we e analysed. A he same ime, a s a is ical e alua ion was ca ied ou , and he e o e he s udy con ains he a e age alues and s anda d de ia ions o all measu ed pa ame e s. The esul s show ha he comp essi e s eng h and he elec ical esis i i y o he su ace and bulk ha e a high co ela ion. In con as , he dynamic modulus and elec ical esis i i y ha e low linea co ela ion, bu i was possible o apply a quad a ic cu e wi h a high deg ee o i . Fo he compa ison o s a ic elas ic modulus and elec ical esis ance, he quali y o he quad a ic eg ession model was low bu su icien . The esul s show ha , o s uc u al conc e e, he p esen ed NDT me hods can be used o es ima e o he pa ame e s ob ained om he DT me hods. Keywo ds: conc e e; NDT; quad a ic eg ession; du abili y; modulus o elas ici y; s eng h; co ela ion analysis 1. In oduc ion Building s uc u es a e a ec ed h oughou hei li e ime by mechanical, dynamic, clima ic, and deg ada ion ac o s [ 1 , 2 ]. All hese aspec s can, o e ime, cause he pa o he s uc u e o become unsa is ac o y in e ms o load-bea ing capaci y o se iceabili y. Due o his, egula inspec ions and quali y con ol a e some o he basic equi emen s o he cons uc ion indus y [ 3 ]. In he e alua ion o building s uc u es, hei cu en condi ion is assessed based on app op ia ely selec ed diagnos ic me hods. Cu en ly, he diagnos ics o building s uc u es a e mainly based on des uc i e me hods. Thei use is no always op imal p ecisely because o he in asi e in e en ion in o he s uc u e. Non-des uc i e es s a e a sui able choice o s uc u es diagnos ics because hey a e as , accu a e, and can be epea ed [4]. The comp essi e s eng h o conc e e is one o he mos impo an a iables in assess- ing he quali y o a s uc u e and should be iewed as a a iable pa ame e . Thus, he e alua ion o he condi ion o exis ing s uc u es is pe o med s anda dly in co e wells and hei de e mina ion o he p esen alue o s eng h [ 5 ]. The e a e also many s udies dealing wi h he analysis o he ela ionship be ween des uc i e and non-des uc i e me hods o de e mining comp essi e s eng h and o he impo an pa ame e s. The mos Ma hema ics 2022,10, 460. h ps://doi.o g/10.3390/ma h10030460 h ps://www.mdpi.com/jou nal/ma hema ics Ma hema ics 2022,10, 460 2 o 13 commonly used non-des uc i e me hod o e i y he quali y o conc e e and de e mine i s comp essi e s eng h is he ebound ha dness es me hod [6]. I is also possible o use he ul asonic e alua ion me hod, which wo ks acco ding o he p inciple o ansmi ing ul asonic wa es o he su ace o he s uc u e by an exci e and hen moni o ing he speed o he ansmi ed pulses [7,8]. The gene al ad an ages o non-des uc i e es ing o s uc u es a e well known, bu he mos impo an a e speed and economy. On he con a y, he accu acy o non-des uc i e es s can be a ec ed by many pa ame e s such as agg ega e g ain size, conc e e age, and wa e coe icien [ 9 – 12 ]. T ykoz e al. [ 13 ] p esen ed e idence o he impo ance o non-des uc i e es ing (NDT) measu emen s in p ac ice in he e alua ion o exis ing conc e e s uc u es. This pape p esen s a co ela ion and eg ession analysis o se e al conc e e pa ame- e s ob ained du ing he ini ial cu ing s age om 1 o 128 days. The selec ed pa ame e s can be used as inpu pa ame e s o he nume ical analysis o he du abili y o ein o ced conc e e s uc u es subjec ed o common o ce and chemical loads [ 14 – 17 ]. These nume ical models a e a ailable in bo h de e minis ic and s ochas ic o ms, and since hey a e com- pu a ionally and ime-consuming, an adequa e desc ip ion o he inpu pa ame e s o he ime a iables is equi ed. The ime-dependen pa ame e s men ioned include comp essi e s eng hs, s a ic modulus o elas ici y, dynamic modulus o elas ici y de i ed om ul a- sonic eloci y [ 18 , 19 ], and su ace and bulk elec ical esis i i y [ 20 – 22 ], which can be used o de e mine he chlo ide di usion pa ame e o conc e e [ 23 ]. In s udies, a compa ison o he esul s o he esis i i y o he su ace and he eloci y o he ul asonic pulse was p esen ed [ 24 , 25 ]. Con en ional conc e e shows he same alues om bo h me hods, e en in agg essi e en i onmen s. The objec i e was o e alua e he simples possible ela ionship be ween wo selec ed pa ame e s, ha is, a linea eg ession equa ion o apply a quad a ic eg ession cu e. Due o he in oduc ion o hese equa ions in u he calcula ions, he linea o m is p e e able, bu i i is no accu a e, a mo e complex polynomial mus be applied. This pape p esen s a basic desc ip ion o heexpe imen al e alua ion, s a is ical and co ela ion analyses, and he esul ing equa ions, accompanied by he deg ee o ag eemen . All o his suppo s he long- e m goals o imp o ing non-des uc i e es ing p ocedu es, using non- adi ional ins umen a ion, and analysing ela ionships be ween he esul s o s anda dised des uc i e me hods. 2. Ma e ials and Me hods Fo he analysis o he ela ionship be ween des uc i e and non-des uc i e me hods o conc e e es ing, a s anda d conc e e based on Po land cemen was chosen, wi h an expec ed s eng h class o C40/50. This conc e e is used in he Czech Republic, among o he hings, o he load-bea ing elemen s o ein o ced conc e e b idge s uc u es [ 26 ]. This ma e ial was chosen o pu ely p agma ic easons, as i is widely used in mode n imes and is no bu dened wi h any chemical addi i es o non-s anda d ing edien s. A he same ime, his conc e e composi ion is ideal o u he ex ension o esea ch whe e he e ec o change in composi ion, non-s anda d admix u es, and o he s can be analysed. 2.1. P ope ies o Conc e e The conc e e mix u e was p epa ed acco ding o he p ac ice o EN 206 + A1 [ 27 ]. The composi ion is shown in Figu e 1. The equi emen was a wa e coe icien w/c = 0.4 and a s eng h class o a leas C40/50. Fo he needs o he expe imen al p og am, conside ing he cu ing o conc e e a he ime, a la ge numbe o samples we e p epa ed. Cubes wi h an edge leng h o 150 mm, la ge cylinde s wi h a diame e o 150 mm and a leng h o 300 mm, and small cylinde s wi h a diame e o 100 mm and a leng h o 200 mm we e p epa ed. The uses o each sample o speci ic es s a e gi en below. The esh conc e e mix was pou ed in o he moulds, and a e an ini ial cu ing pe iod o 24 h, he samples we e demoulded. The s o age o all samples was managed unde labo a o y condi ions o a oid undesi able deg ada ion. The es s we e pe o med 7, 28, 63, and 126 days a e conc e ing. Acco ding o s anda ds, i was necessa y o use 3 samples o each ype o es and each Ma hema ics 2022,10, 460 3 o 13 ime. Due o his, a leas 12 samples o e e y me hod we e p epa ed a he beginning. Fo he non-des uc i e es s, his need was no p esen , and he same 3 samples we e es ed a each ime. Figu e 1. Conc e e mix u e p ope ies; amoun pe 1 m2[kg]. 2.2. Des uc i e Tes ing Me hods Fo he p esen esea ch, wo s anda d me hods o labo a o y es ing o conc e es we e selec ed, namely a es o de e mine he comp essi e s eng h on cubes and a es o de e mine he s a ic modulus o elas ici y om ul asonic measu emen s. The comp essi e s eng h was es ed acco ding o EN 12390-3 [ 28 ] on h ee cubes se e al imes-7, 28, 63, and 126 days a e conc e ing. The es was ca ied ou on a s anda d hyd aulic p ess machine, and he cubic s eng hs o he conc e e we e calcula ed om he maximum o ce and he load a ea eco ded. The s a ic modulus o elas ici y in he comp ession o ha dened conc e e exp esses he dependence be ween he s ess and he s ain ha a gi en elemen o s uc u e exhibi s unde s ess. The p ocedu e o de e mine he s a ic comp essi e modulus o elas ici y o conc e e is de ined in ISO 1920-10 [ 29 ]. The de e mina ion o he s a ic modulus o elas ici y was ca ied ou by cyclic loading o he es pieces in a p ess, which was ca ied ou acco ding o EN 12390-13 [30]. 2.3. Non-Des uc i e Tes ing Me hods Th ee small cylinde s wi h a diame e o 100 mm and a leng h o 200 mm and h ee la ge cylinde s wi h a diame e o 150 mm and a leng h o 300 mm we e p epa ed o he NDT me hods. Two ypes o cylinde s we e chosen o analyse he e ec o he shape and size o he sample on he esis i i y o he su ace. A Wenne p obe [ 31 ] (see Figu e 2) was used o measu e he elec ical esis i i y o he su ace. The es was ca ied ou on six cylind ical samples ( h ee small and h ee la ge) acco ding o he AASHTO T358 s anda d [ 32 ]. Su ace esis ance was measu ed om ou longi udinal sides, and hen he mean alue and s anda d de ia ion we e de e mined. The su ace esis i i y was hen con e ed o an adequa e bulk esis i i y using a calib a ion ela ionship dependen on he dimensions o he sample acco ding o p e iously published p ocedu es [33]. Ma hema ics 2022,10, 460 4 o 13 Figu e 2. A Wenne p obe be o e he measu emen . An CON me e [ 34 ] was used o measu e he bulk elec ical esis i i y. This es was also ca ied ou on six cylind ical samples ( h ee small and h ee la ge) acco ding o ASTM C1876 [ 35 ]. Fu he mo e, an ul asonic pulse me hod was used o de e mine he dynamic modulus o elas ici y acco ding o EN 12504-4 [ 7 ]. The dynamic modulus o elas ici y was de e mined om he bulk densi y o conc e e and he ime o ul asound passage h ough he sample. The es was pe o med on h ee la ge cylind ical samples. 2.4. Co ela ion and Reg ession Analysis Since all es s we e pe o med on specimens a he same ime pe iods since conc e ing, he ela ionship be ween he esul s o des uc i e and non-des uc i e me hods could be analysed. When looking o a ela ionship be ween wo se s o esul s, he co ela ion coe - icien can be used a he i s le el. The p esen ed esea ch shows he Pea son co ela ion coe icien (PCC), which is one o he mos widely used [ 36 ]. The PCC shows he deg ee o linea co ela ion be ween wo se s o da a. I he alue is close o 1 (o − 1) he e is a possible high linea co ela ion (posi i e o +1 and nega i e o − 1). On he o he hand, i i app oaches 0, i is no possible o alk abou a linea co ela ion. PCC p o ides a basic iew o he da a se s bu can de ini ely help o u he analysis. The nex s ep in assessing he ela ionship be ween he selec ed ou comes was o in oduce a poin se consis ing o one se o da a on he X-axis and ano he se o da a ela ed o he same ime on he Y-axis. The poin s depic ing he measu ed alues we e hen i ed wi h a line segmen showing he s anda d de ia ion. This p ocedu e hen allows he sea ch o a linea eg ession equa ion o , i he i is low, a quad a ic eg ession equa ion ha uses a pa abola [ 37 ]. In ei he case, i is necessa y o e alua e g aphically and ma hema ically how closely he line o pa abola i s he se o measu ed alues. The coe icien is use ul o de e mine he bes i [ 38 ]. The coe icien o de e mina ion shows he i be ween he measu ed alues and he chosen cu e. The limi s o R 2 a e a ied. Fo example, a alue o 0.82 o 1 is epo ed o indica e a e y s ong i , a alue o 0.5 o 0.81 is a s ong i , and lowe alues a e mode a e o weak i s [ 39 ]. The e o e, he alue o 0.8 was chosen as he bounda y whe e linea co ela ion is su icien , and he e is no need o look o a quad a ic equa ion. 3. Resul s The ollowing sec ions show he esul s o all measu emen s and hen he indi idual co ela ions and eg essions on he 10 pai s o esul s. The g aphs con ain a ma hema ical desc ip ion o he linea o quad a ic eg ession cu e and he alues o R 2 . Fu he analysis o he esul s was pe o med a he le el o applica ion o linea eg ession and bes - i anal- Ma hema ics 2022,10, 460 5 o 13 ysis using he coe icien o de e mina ion. In case o low ag eemen , quad a ic eg ession was applied. 3.1. Time-Dependen Resul s Due o he chosen p ocedu e o measu ing all pa ame e s in se e al ime s eps, i is possible o display he esul s oge he on one g aph and look o p ima y ela ionships. Figu e 3shows he g aph o he elec ical esis i i y measu ed in small and la ge cylinde s om bo h su ace and bulk ins umen s. The same g aph in he igu e also shows a plo o he inc ease in comp essi e s eng h alues on he cubes. The i s iew o eshadows a ela ionship ha could be u he e alua ed. Figu e 3. Time-dependen esul s o elec ical esis i i y and comp essi e s eng h. The nex g aph (Figu e 4) again shows he same elec ical esis i i y alues bu adds he s a ic and dynamic modulus alues a he gi en imes. The li e a u e indica es ha he s a ic modulus co esponds o app oxima ely 60% o he dynamic modulus [ 40 ]. This ac is also obse ed he e. Figu e 4. Time-dependen esul s o elec ical esis i i y and modulus o elas ici y. The Pea son co ela ion coe icien desc ibed abo e was chosen as he i s nume ical esul o he analysis. Table 1shows he esul s o his coe icien o each pai o esul s. I can be seen ha he elec ical esis i i y has an almos 100% co ela ion when compa - ing su ace and bulk measu emen s. The co ela ion be ween comp essi e s eng h and elec ical esis ance anges om 0.94 o 0.96. The o he co ela ions a e a o below 0.8. Ma hema ics 2022,10, 460 6 o 13 Table 1. Resul s o he nume ical analysis based on Pea son’s co ela ion coe icien (PCC). Fi s Pa ame e Second Pa ame e PCC Small cylinde su ace elec ical esis i i y Small cylinde bulk elec ical esis i i y 0.99 La ge cylinde su ace elec ical esis i i y La ge cylinde bulk elec ical esis i i y 0.99 Comp essi e s eng h Small cylinde bulk elec ical esis i i y 0.96 Comp essi e s eng h La ge cylinde bulk elec ical esis i i y 0.94 Comp essi e s eng h Dynamic modulus o elas ici y 0.85 Comp essi e s eng h S a ic modulus o elas ici y 0.78 Dynamic modulus o elas ici y Small cylinde bulk elec ical esis i i y 0.77 Dynamic modulus o elas ici y La ge cylinde bulk elec ical esis i i y 0.68 S a ic modulus o elas ici y Small cylinde bulk elec ical esis i i y 0.75 S a ic modulus o elas ici y La ge cylinde bulk elec ical esis i i y 0.65 3.2. Bulk and Su ace Elec ical Resis i i y Fo he i s esul s, i.e., su ace and bulk elec ical esis i i y on small and la ge cylinde s, a high ag eemen o linea dependence can be obse ed (see Figu e 5). The esul s show ha i is no necessa y o look o disc epancies in he Wenne p obe and Con measu emen s o he p epa ed conc e e ype. The e o e, only he bulk esis i i ies we e used o u he e alua ion. Figu e 5. Linea eg ession analysis o he ela ionship be ween su ace and bulk elec ical esis i i y on la ge and small cylind ical samples (LC = La ge Cylinde s, SC = Small Cylinde s). 3.3. Comp essi e S eng h s. Elec ical Resis i i y The ela ionship be ween he conc e e s eng h ob ained om he cubic es and he elec ical esis i i y measu ed in la ge and small cylinde s using linea eg ession is shown in Figu e 6. The coe icien o de e mina ion alues o bo h se s a e high, 0.89 o he la ge cylinde s and up o 0.93 o he small cylinde s. Thus, i can be concluded ha he ime dependence o bo h pa ame e s is almos linea , which suppo s he elec ical esis i i y measu emen as an al e na i e NDT me hod o de e mining he comp essi e s eng h o conc e e. I is possible o use linea eg ession cu es o nume ical modelling. Ma hema ics 2022,10, 460 7 o 13 Figu e 6. Linea eg ession analysis o he ela ionship be ween bulk elec ical esis i i y and com- p essi e s eng h (LC = La ge Cylinde s, SC = Small Cylinde s). 3.4. Comp essi e S eng h s. Modulus o Elas ici y The ela ionship be ween comp essi e s eng h and modulus o elas ici y was also in es iga ed. Bo h he s a ic modulus ob ained om des uc i e es ing (DT) and he dy- namic modulus ob ained om NDT ul asonic p opaga ion eloci y es ing we e e alua ed. Figu e 7shows he plo s o he linea eg ession be ween he pa ame e s. The coe icien o de e mina ion has medium alues. Figu e 7. Linea eg ession analysis o he ela ionship be ween modulus o elas ici y and comp essi e s eng h (D = Dynamic, S = S a ic). The e o e, he quad a ic eg ession and i s i o bo h se s o assessed esul s we e analysed (see Figu e 8). The ela ionship be ween he s a ic modulus and he comp essi e s eng h o he conc e e also shows he di e gence in his case, which is p obably due o he non-uni o m beha iou o he s a ic modulus o e ime. On he o he hand, when he quad a ic cu e is applied o he pai o comp essi e s eng h and dynamic modulus, he alue o he coe icien o de e mina ion is 0.85, again showing high ag eemen . Ma hema ics 2022,10, 460 8 o 13 Figu e 8. Quad a ic eg ession analysis o he ela ionship be ween modulus o elas ici y and comp essi e s eng h (D = Dynamic, S = S a ic). 3.5. Dynamic Modulus o Elas ici y s. Elec ical Resis i i y The o e all e alua ion included he analysis o wo se s o esul s om NDT mea- su emen s, namely, dynamic modulus o elas ici y de i ed om ul asonic eloci y and elec ical esis i i y. Linea eg ession is p epa ed in Figu e 9 o he combina ion o la ge and small cylinde s ha we e used o he elec ical esis ance measu emen s. The alues o he coe icien s o de e mina ion a e low, below 0.6, so i can be concluded ha he e is a small linea ela ionship. Figu e 9. Linea eg ession analysis o he ela ionship be ween bulk elec ical esis i i y and dynamic modulus o elas ici y (LC = La ge Cylinde s, SC = Small Cylinde s). As in he p e ious case, he nex s ep was o apply a quad a ic eg ession cu e, which could show a highe i . Thus, in Figu e 10, i can be seen ha , indeed, he quad a ic eg ession p o ides unexpec edly high goodness o i o bo h cases. Thus, he change in he measu ed elec ical esis i i y and ul asonic eloci y pa ame e s is highly simila o e ime and can be al e na ed o he conc e e ype e alua ed he e. Ma hema ics 2022,10, 460 9 o 13 Figu e 10. Quad a ic eg ession analysis o he ela ionship be ween bulk elec ical esis i i y and dynamic modulus o elas ici y (LC = La ge Cylinde s, SC = Small Cylinde s). 3.6. S a ic Modulus o Elas ici y s. Elec ical Resis i i y Ano he pai , his ime om DT and NDT measu emen s, is s a ic modulus e sus elec ical esis i i y on small and la ge cylinde s. In he i s s age, he linea cu e was applied again (see Figu e 11). Howe e , i showed a low ag eemen , al hough he coe icien o de e mina ion o he small cylinde s was almos 0.73. Figu e 11. Linea eg ession analysis o he ela ionship be ween bulk elec ical esis i i y and dynamic modulus o elas ici y (LC = La ge Cylinde s, SC = Small Cylinde s). I was expec ed ha a quad a ic eg ession, which was app op ia e o some o he p e ious me hods, would gi e much be e esul s. The quad a ic cu e analysis o he s a ic modulus and elec ical esis i i y is shown in Figu e 12. He e again, di e en alues can be seen o la ge and small cylinde s. Howe e , in his case, he quad a ic eg ession imp o ed he alue o he coe icien o de e mina ion o small cylinde s o only 0.87, bu o la ge cylinde s, his alue was inc eased o 0.78. Bo h alues a e signi ican ly highe han o linea eg ession and demons a e some ag eemen be ween he esul s o he wo me hods.