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High K Bands in Mid-Supershell Nuclei

Butler, P. A.,Humphreys, R. D.,Greenlees, P. T.,Herzberg, R.-D.,Jenkins, D. G.,Jones, G. D.,Kankaanpää, H.,Kettunen, H.,Rahkila, P.,Scholey, C.,Uusitalo, J.,Amzal, N.,Andreoiu, C.,Andreyev, A,Appelbe, D.,Bastin, J. E.,Brew, P. M. T.,Eskola, K.,Freeman, S

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This is a self-archived version of an original article. This version may differ from the original in pagination and typographic details. Author(s): Title: Year: Version: Copyright: Rights: Rights url: Please cite the original version: CC BY 4.0 https://creativecommons.org/licenses/by/4.0/ High K Bands in Mid-Supershell Nuclei © 2003 Jagellonian University Published version Butler, P. A.; Humphreys, R. D.; Greenlees, P. T.; Herzberg, R.-D.; Jenkins, D. G.; Jones, G. D.; Kankaanpää, H.; Kettunen, H.; Rahkila, P.; Scholey, C.; Uusitalo, J.; Amzal, N.; Andreoiu, C.; Andreyev, A; Appelbe, D.; Bastin, J. E.; Brew, P. M. T.; Eskola, K.; Freeman, S. J.; Gerl, J.; Hammond, N. J.; Hauschild, K.; Helariutta, K.; Hessberger, F.-P.; Huerstel, A.; Ikin, P. J. C.; Jones, P. M.; Joss, D. T.; Julin, R.; Juutinen, S.; Keenan, A.; Khoo, T.-L.; Korten, W.; Kuusiniemi, P.; Le Coz, Y.; Leino, M.; Leppänen, A.-P.; Muikku, M.; Nieminen, P.; Odegard, S. W.; Page, R. D.; Page, T.; Pakarinen, J.; Reiter, P.; Simpson, J.; Sletten, G.; Theisen, Ch.; Varley, B. J.; Wollersheim, H.-J. Butler, P. A., Humphreys, R. D., Greenlees, P. T., Herzberg, R.-D., Jenkins, D. G., Jones, G. D., Kankaanpää, H., Kettunen, H., Rahkila, P., Scholey, C., Uusitalo, J., Amzal, N., Andreoiu, C., Andreyev, A., Appelbe, D., Bastin, J. E., Brew, P. M. T., Eskola, K., Freeman, S. J., . . . Wollersheim, H.-J. (2003). High K Bands in Mid-Supershell Nuclei. Acta Physica Polonica B, 34(4), 2107-2117. https://www.actaphys.uj.edu.pl/R/34/4/2107 2003 Vol. 34 (2003) ACTA PHYSICA POLONICA B No 4 HIGH K BANDS IN MID-SUPERSHELL NUCLEI  P.A. Butler a , R.D. Humphreys a , P.T. Greenlees b R.-D. Herzberg a , D.G. Jenkins a , G.D. Jones a , H. Kankaanpää b H. Kettunen b , P. Rahkila b , C. Sholey a ; b , J. Uusitalo b N. Amzal a , C. Andreoiu a , A. Andreyev a , D. Appelbe j J.E. Bastin a , P.M.T. Brew a , K. Eskola  , S.J. Freeman k , J. Gerl d N.J. Hammond a , K. Haushild e , K. Helariutta d F.-P. Heÿberger d , A. Hürstel e , P.J.C. Ikin a , P.M. Jones b D.T. Joss j , R. Julin b , S. Juutinen b , A. Keenan b , T.-L. Khoo f W. Korten e , P. Kuusiniemi b , Y. Le Coz e , M. Leino b A.-P. Leppänen b , M. Muikku b , P. Nieminen b , S.W. Ødegård g R.D. Page a , T. Page a , J. Pakarinen b , P. Reiter h , J. Simpson j G. Sletten i , Ch. Theisen e , B.J. Varley k , and H.-J. Wollersheim d a Oliver Lo dge Lab oratory, University of Liverp o ol, Liverp o ol L69 7ZE, U.K. b Department of Physis, University of Jyväskylä, FIN-40014 Jyväskylä, Finland  Dept. of Phys. Si., University of Helsinki, FIN-00014 Helsinki, Finland d GSI, D-64291 Darmstadt, Germany e DAPNIA/SPhN CEA-Salay, F-91191 Gif-sur-Yvette, Frane f Argonne National Lab oratory, Argonne, Illinois 60439, USA g Department of Physis, University of Oslo, N-0316 Oslo, Norway h Ludwig Maximilians Universität, D-85748 Garhing, Germany i Niels Bohr Institute, 2100 Cop enhagen, Denmark j CLRC Daresbury Lab oratory, Warrington WA4 4AD, U.K. k Shuster Lab oratory, University of Manhester, Manhester M13 9PL (Reeived November 12, 2002) The sp etrum of prompt onversion eletrons emitted by exited 254 No nulei has b een measured, revealing disrete lines arising from transitions within the ground state band. A striking feature is a broad distribution that p eaks near 100 keV and omprises high multipliity eletron asades, probably originating from M 1 transitions within rotational bands built on high K states. Evidene for the existene of isomeri states in 254 No is presented. PACS numb ers: 21.10.k, 23.20.Lv, 23.20.Nx, 23.60.+e  Presented at the XXXVI I Zakopane Sho ol of Physis Trends in Nulear Physis, Zakopane, Poland, September 310, 2002. (2107) 2108 P.A. Butler et al. 1. Intro dution The understanding of the struture of the heaviest elements, in partiular sup erheavy elements (SHE), is essential for the development of mean eld theories that are used to predit nulear prop erties far from stability (for reviews see [1, 2℄). Exp erimental insight into the struture of sup erheavy nulei an b e obtained by diret measurement of the ground state prop erties of nulei (for review, see [3℄). Attempts to reah the spherial SHE have b een rep orted reently in whih the observation of  -deay from nulei with Z = 114 , 116 and N = 174 , 176 with lifetimes of the order of seonds has b een laimed [4, 5℄. Equally imp ortant information an ome from the study of mid-shell deformed nulei, sine seleted single partile orbitals that lie lose to the spherial shell gap in SHE are lose to the Fermi level in nulei having large quadrup ole deformation. Suh information an ome from radioative deay sp etrosopy or from in-b eam sp etrosopy. In the latter tehnique the prompt deay pro ess is tagged by detetion of the reoiling nuleus or by alpha deay from the reoil (RDT), using eletromagneti separators. In this manner, in-b eam  -ray sp etrosopy has enabled the rotational b ehavior of the even-even nulei 252 No [6℄ and 254 No [79℄ to b e studied up to spin 20 ~ . In these exp eriments the reation pro duts, although p opulated with small ross setions (   3  barn), have b een separated from the dominant ssion bakground. The measurements onrmed that nulei having Z  100 and N  150 have ground state deformation of   0 : 3 . It is exp eted that these nulei are the homologues of neutron rih Er-Hf in the lower osillator shell where rotational bands built on high K states are observed. The quantiation of the struture of these states will b e imp ortant for xing the parameters of mo dels used to predit SHE prop erties. We rep ort here a new exp erimental metho d that an reveal information on heavy nulei additional to that obtained from gamma-ray sp etrosopy. Our tehnique allows the diret detetion of internal onversion eletrons, emitted at the target, in a broad-range, high eieny eletron sp etrometer. The eletrons an b e tagged by reoil detetion or using RDT. The sensitivity of the tehnique is demonstrated here by applying it to the measurement of the low-lying transitions in the ground state band of 226 U, whih are easily observed in a relatively short running time, and to a study of onverted transitions in 254 No, for whih the 4 + ! 2 + up to the 10 + ! 8 + transitions were observed. These studies reveal a striking dierene in the bakground of unresolved transitions for the two reations. We hyp othesize that this arises from the exp eted presene of highK multi-quasipartile states near the Fermi surfae in 254 No. High K Bands in Mid-Supershel l Nulei 2109 2. In-b eam eletron sp etrosopy: SACRED The eletron sp etrometer, SACRED [10℄, employs a single Si PIN wafer, 500 mirons thik, segmented into 25 pixels onneted to individual ampli- ation and timing hannels. The geometry is irular, with 6 annuli, divided into quadrants, surrounding the entral element. The outer diameter of the detetor is 28 mm. Eletrons are transp orted from the target to the detetor using a solenoidal magneti eld of maximum ux density 0.3 T generated by 4 separated, normal onduting oils. The target-detetor distane is 540 mm. The b eam axis is at an angle of 2.5 Æ to the eld axis, interseting at the target p osition. This arrangement has the advantage of having an approximately ollinear geometry, while ensuring that the b eam is displaed by 25 mm from the eld axis at the (upstream) detetor p osition. The resp onse of the detetor to onversion eletrons emitted in the deay of a 133 Ba soure is shown in gure 1. The absolute eieny is ab out 10% for energies < 350 keV. For in-b eam measurements the delta eletron bakground is redued to an aeptable level by an eletrostati barrier plaed b etween the target and the detetor. Further details of the mehanial onstrution are given in Ref. [11℄. 0 50 100 150 200 250 300 10 3 10 4 10 5 10 6 counts/2keV test X Axis Title electron energy (keV) Fig. 1. Sp etrum of 133 Ba soure, showing the detetor resp onse on a logarithmi sale. The ollinear geometry, while oering the advantage of reduing b oth Doppler broadening of the eletron lineshap e and the delta eletron ux in the bakward diretion, enabled the eletron sp etrometer to b e oupled to the gas-lled reoil separator RITU [12℄. The reoil pro duts were transp orted in RITU to a 16-fold segmented and resistive silion pad detetor at its fo al plane. This detetor is divided into approximately 200 pixels. 2110 P.A. Butler et al. The magnet volume of RITU and the setion of SACRED ontaining the target are lled with 0.3 and 0.7 mbar helium gas for reations indued by A  20 and A  50 pro jetiles resp etively. This volume is separated from the remaining volume of SACRED by two 60  g/m 2 arb on foils of 15 mm radius and 170 mm separation with pump ed intermediate volume. In this way the pressure of the region ontaining the barrier and the detetor was maintained at ab out 10  6 torr, thus reduing the bakground from aelerated eletrons pro dued following ionization of the residual gas moleules by the b eam. The energy loss of 50150 keV eletrons in the target and foils is 11.5 keV. 3. Conversion eletron measurements in 226 U These exp eriments were arried out at the aelerator lab oratory of the University of Jyväskylä. In the rst exp eriment a 10 partile nA b eam of 111 MeV 22 Ne (orreting for energy loss in the arb on foils) b ombarded a 208 Pb target of thikness 200  g/m 2 for approximately 25 h. In this exp eriment the p otential of the eletrostati barrier was  35 kV with resp et to target and detetor. The onversion eletron sp etrum of 226 U, pro dued in the   6  b 4 n hannel, is shown in gure 2(a). It was obtained by requiring that the detetion of any eletron at the target using SACRED b e aompanied by the detetion of reoils in the fo al plane detetor of RITU within a time window of  50 ns of their arrival at the fo al plane. The reoils are identied by requiring that there is an alpha deay of energy range 7.497.63 MeV within 800 ms in the same pixel of the implantation detetor. There were 1280 tagged reoils deteted in this exp eriment. Figure 2(b) shows a simulated sp etrum obtained using the Monte Carlo program desrib ed in Ref. [10℄, orresp onding to the same numb er of reoils as observed exp erimentally. The simulation assumes that the observed onversion eletrons only arise from transitions previously observed in an array of  -ray sp etrometers and identied using the RDT tehnique [13℄. More details of the onversion eletron exp eriment and its results, in partiular the rst rm assignment of the energy of the 2-0 transition, are given in Ref. [14℄. It is evident from omparison of the exp erimental and simulated sp etrum that the exess bakground observed over that a- ounted for by the simulation is quite small. The simulation takes into aount the transp ort of the eletrons in the magneti and eletri elds, sattering in or from the detetor, energy sharing at the pixel b oundaries, and threshold eets. High K Bands in Mid-Supershel l Nulei 2111 0 50 100 150 200 250 300 0 20 40 Y Axis Title electron energy (keV) b) 0 20 2 0 42 L M L M counts/2keV X Axis Title a) Fig. 2. (a): Exp erimental onversion eletron sp etrum (orreted for the ontribution from random oinidenes) tagged by the harateristi  -deay of 226 U. In this sp etrum the energies are not orreted for Doppler shift. Transitions in the ground state band are identied. (b): Simulated sp etrum for 226 U as desrib ed in the text. 4. Measurement of high multipliity ontinuum in 254 No In a seond exp eriment a b eam of 219 MeV 48 Ca was employed. In this ase the average b eam energy in the enter of the 208 Pb target (216 MeV) orresp onds to the maximum of the yield of the reation 208 Pb( 48 Ca, 2 n ) 254 No. Targets of thiknesses 250  g/m 2 and 400  g/m 2 of enrihment 98% 208 Pb were eah b ombarded by a b eam of 1.53 partile nA for approximately 110 h eah. The p otential of the eletrostati barrier was  40 kV. Figure 3(a) shows the total eletron sp etrum tagged by the detetion of fusion pro duts. In this ase it is not neessary to verify that the reoils are 254 No by measuring their alpha deay as there are no other omp eting omp ound nuleus hannels: the ombined p opulation of 253 ; 255 No is  1 % of that of 254 No [15, 16℄. The eletron sp etrum whih is tagged by the subsequent deay of 2112 P.A. Butler et al. 0 50 100 150 200 250 300 0 50 100 electron energy (keV) d) 0 10 20 c) g 0 25 50 counts/2keV b) 0 25 50 L M 10 8 8 6 L M 6 4 L M 4 2 L M a) Fig. 3. (a): The exp erimental onversion eletron sp etrum tagged by 254 No re- oils, orresp onding to any number of eletrons deteted in SACRED (solid b old line). In this sp etrum the energies are not orreted for Doppler shift. The lowest transitions in the ground state band are identied. Also shown are the simulated sp etra as desrib ed in the text for g K = 0 (hashed area with solid line b order) and for g K  g R = 0 (dashed line). (b): as (a) exept that exp eriment and simulation orresp ond to the detetion of a single eletron. (): Spetrum of seond eletron in oinidene with a seleted region (labelled `g') of energy for the rst eletron, tagged by reoils (solid b old line). Also shown is the exp erimental spe- trum tagged by  -deay for any numb er of eletrons deteted (dashed line). (d): eletron sp etrum taken in random oinidene. High K Bands in Mid-Supershel l Nulei 2113 alpha partiles in the energy range 8.04 to 8.15 MeV, with a searh time of 600 s (see dashed line in gure 3()), has approximately half the total ounts, as exp eted. We were able to distinguish evap oration residues, target-like re- oils, sattered b eam and radioative deay pro duts by employing a parallel plate prop ortional ounter in front of the silion implantation detetor. Two features are apparent from gure 3(a). First, the onversion ele- trons orresp onding to transitions in the ground state rotational band up to spin 10 in 254 No are identiable (the struture observed at  65 and 105 keV arises from hitherto unidentied transitions in 254 No). The details of these measurements, in partiular the rst diret measurement of the energy of the 42 transition, are given in Ref. [14℄. The seond notieable feature is the pronouned bakground, entered at around 100 keV. The intensity of this bakground is muh larger than the bakground observed in the sp etrum orresp onding to 226 U transitions (gure 2(a)). The most interesting prop erty of the bakground is that it has a muh higher eletron multipliity than that of the disrete transitions. This is demonstrated by demanding that the sp etrum is only inremented if no other eletrons are deteted in any of the SACRED pixels within 100 ns of the detetion of the rst eletron. The resulting sp etrum is shown in gure 3(b) in whih the p eak to bakground is signiantly improved. The simulation o de an b e used to roughly estimate the mean eletron multipliity, as it provides an aurate mo del of the resp onse of the SACRED sp etrometer. It remains to mo del the mehanism by whih the entry states in 254 No dep opulate and emit onversion eletrons. The simplest mo del is to assume that only the ground state band is p opulated, so that there is no other soure of onversion eletrons. In this ase the relative intensities of the transitions feeding the 4 + state are taken from the gamma-ray measurements [8, 9℄. The present measurements indiate that the intensity of the 64 and the 42 transitions are the same [14℄, and these are assumed to b e the same as that of the 20 transition. The measured yield of the 64 L transition in the ground state band is 126  18 for a single eletron deteted, 160  30 for any numb er of eletrons deteted (ratio R (6  4) = 0 : 78  0 : 16 ), for a total of 7150 re- oils. In the simulation, arried out for four times the numb er of reoils to that reorded in the measurement, the values for the yield of the 64 transition are resp etively 1280 and 1530 ( R (6  4) = 0 : 84 ). The measurements are onsistent with the simulation if ab out 40% of the p opulation of 254 No passes through the lowest transitions. On average 3.7 eletrons are emitted simultaneously in this deay path, inluding the undeteted 20 transition. In order to mo del the bakground, we assumed that this arises from de- ays within a single rotational band built on a K = 8 isomeri bandhead and p opulated with the same entry spin distribution as that measured for all states by Reiter et al. [9℄. The value of g K is taken to b e 0, with g R = 0 : 3 . 2114 P.A. Butler et al. For this band we assumed a onstant moment of inertia of 100 ~ 2 MeV  1 , slightly larger than that of the highest transitions in the ground state band (this allows a b etter t to the low energy part of the sp etrum). The ele- tron energies are then randomized by applying a gaussian distribution of  = 10 keV, to aount for the presene of many suh bands having differing moments of inertia. The alulated sp etrum, also arried out for 28,600 reoils as for the previous simulation and then renormalised by a fator of 0.10, is shown also in gure 3(a). The measured intensity of the bakground mathes the alulated intensity, implying that approximately 40% of all deteted reoils pro eed through these paths. The exp eted values of g K for the lowest 2 quasi-partile K  = 8  bands in 254 No are   0 : 3 ( 9 2  [734℄  7 2 + [613℄  , Ref. [17℄), 0 ( 9 2  [734℄  7 2 + [624℄  , Ref. [18℄) and 1 ( 9 2 + [624℄  7 2  [514℄  , Refs. [17, 18℄). For this range of values of g K the alulated ratio of integrated ounts for single and any eletron deteted ( R bkg ) is 0.570.59, similar to the measured value of 0 : 58  0 : 03 . The orresp onding value of the mean eletron multipliity for these paths is in the range 78. In the extreme ase when ( g K  g R ) = 0 (purely eletri transitions) the al- ulated value of R bkg is 0.64, orresp onding to an eletron multipliity of 4 distributed evenly b etween I ! I  1 and I ! I  2 transitions. In this ase the alulated sp etrum overestimates the high energy part of the sp etrum (see dashed line in gure 3(a),(b)). If it is assumed that the bandhead is not isomeri, so that the K = 8 state deays immediately to the 8 + memb er of the ground state band, then the value of R bkg for g K = 0 is 0.47 (multipliity 10). This feeding pattern annot b e signiant, as demonstrated in gure 3() whih shows the sp etrum of eletrons in oinidene with a seleted region of the bakground. Finally, we have to onsider the p ossibility that the bakground is largely atomi in origin and that it arises from the atomi ollisions of the reoiling nob elium atoms with the Pb atoms in the target. We b elieve that this p ossibility is unlikely as the bakground has a very dierent shap e to that arising from the delta bakground pro dued by ollisions of b eam partiles with the target. Figure 3(d) shows the eletron sp etrum taken in random oinidene, whih is idential in sp etral shap e to the singles sp etrum. It p eaks in intensity at an energy that is lose to the barrier voltage. In addition, we ompared the integral bakground yield p er nob elium reoil deteted for when the target thikness was 250  g/m 2 (4710 reoils) and when the target thikness was 400  g/m 2 (2440 reoils). The measured values were very similar, 0 : 177  0 : 008 and 0 : 170  0 : 010 , resp etively. If the bakground arose from No+Pb atomi ollisions it might b e exp eted that the yield would sale with the target thikness.